skip to content

Department of Veterinary Medicine Research Facilities

 

Making the most of over 25 years of experience in quantitative elemental analysis by inductively couple plasma (ICP) techniques to answer bio-clinical and environmental research questions, the Trace Element Analysis Facility offers expert advice to research groups and companies on quantitative element analysis, as well as sample preparation and analysis on a collaborative or fee-for-service basis. 

To discuss any aspect of these services, please contact icp@vet.cam.ac.uk

What we offer

  • Elemental/isotopic analysis
  • Single particle analysis
  • Single or multi-elements 
  • Semi- and full-quantitative analysis
  • Heavy metals analysis
  • Impurity analysis

Samples we routinely analyse

  • Water, foods and feeds
  • Materials and minerals
  • Whole blood, serum/plasma, urine, skin, bone, intestinal and other tissues
  • Pharmaceuticals
  • Samples from in vitro assays

Analytical concentration range

ppt (ng/L) to ppm (mg/L) - depending on element and sample type

Core instruments

Current state-of-the-art Agilent triple quadrupole inductively coupled plasma mass spectrometer (8900 ICP-MS/MS) and Horiba Jobin Yvon inductively coupled plasma optical emission spectrometer (Ultima 2c).  

The latest microwave digestion technology in the Milestone UltraWave single reaction chamber microwave digestion system.

All housed in a clean and purpose designed trace element room.

Sample prep requirement

Liquid/aqueous samples should ideally be acidified (1-5%  nitric acid) to keep elements (metals) in solution.

Solid specimens should be destructed with nitric acid or in combination with hydrogen peroxide. The final solutions for analysis should ideally contain 1% nitric acid and < 0.2% dissolved salts/solid matter.

We offer advice on sample preparation (i.e. digestion) and/or provide the complete sample prep and analysis package. Please contact us to discuss further. 

Indicative cost

From £7 to £27 per sample, however this depends on the number and frequency of samples, instrument, number of elements and sample prep requirements.